MARC details
| 000 -LEADER |
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| fixed length control field |
04950cam a2200373 i 4500 |
| 001 - CONTROL NUMBER |
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| control field |
17894990 |
| 005 - DATE AND TIME OF LATEST TRANSACTION |
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| control field |
20210112112710.0 |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION |
|---|
| fixed length control field |
130923s2018 flua bf 001 0 eng |
| 010 ## - LIBRARY OF CONGRESS CONTROL NUMBER |
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| LC control number |
2013443454 |
| 020 ## - INTERNATIONAL STANDARD BOOK NUMBER |
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| International Standard Book Number |
9781439860977 (paperback) |
| 040 ## - CATALOGING SOURCE |
|---|
| Original cataloging agency |
DLC |
| Language of cataloging |
eng |
| Description conventions |
rda |
| Transcribing agency |
DLC |
| Modifying agency |
DLC |
| 042 ## - AUTHENTICATION CODE |
|---|
| Authentication code |
pcc |
| 050 00 - LIBRARY OF CONGRESS CALL NUMBER |
|---|
| Classification number |
QD251.3 |
| Item number |
.L46 2013 |
| 082 00 - DEWEY DECIMAL CLASSIFICATION NUMBER |
|---|
| Classification number |
547.0078 |
| Edition number |
23 |
| Item number |
L.J.A |
| 100 1# - MAIN ENTRY--PERSONAL NAME |
|---|
| Personal name |
Leonard, J. |
| Fuller form of name |
(John), |
| Dates associated with a name |
1954- |
| Relator term |
author. |
| 245 10 - TITLE STATEMENT |
|---|
| Title |
Advanced practical organic chemistry / |
| Statement of responsibility, etc |
John Leonard, Barry Lygo, Garry Procter. |
| 250 ## - EDITION STATEMENT |
|---|
| Edition statement |
Third edition / |
| Remainder of edition statement |
John Leonard, Barry Lygo, Garry Procter. |
| 264 #1 - PUBLICATION, DISTRIBUTION, ETC. (IMPRINT) |
|---|
| Place of publication, distribution, etc |
Boca Raton : |
| Name of publisher, distributor, etc |
CRC Press, Taylor & Francis Group, |
| Date of publication, distribution, etc |
[2018] |
| 300 ## - PHYSICAL DESCRIPTION |
|---|
| Extent |
xxv, 330 pages : |
| Other physical details |
illustrations ; |
| Dimensions |
24 cm |
| 336 ## - CONTENT TYPE |
|---|
| Content type term |
text |
| Source |
rdacontent |
| 337 ## - MEDIA TYPE |
|---|
| Media type term |
unmediated |
| Source |
rdamedia |
| 338 ## - CARRIER TYPE |
|---|
| Carrier type term |
volume |
| Source |
rdacarrier |
| 504 ## - BIBLIOGRAPHY, ETC. NOTE |
|---|
| Bibliography, etc |
Includes bibliographical references and index. |
| 505 0# - FORMATTED CONTENTS NOTE |
|---|
| Formatted contents note |
General introduction<br/><br/>Safety<br/>Safety is your primary responsibility<br/>Safe working practice<br/>Safety risk assessments<br/>Common hazards<br/>Accident and emergency procedures<br/>Bibliography<br/><br/>Keeping records of laboratory work<br/>Introduction<br/>The laboratory notebook<br/>Keeping records of data<br/>Some tips on report and thesis preparation<br/>References<br/><br/>Equipping the laboratory and the bench<br/>Introduction<br/>Setting up the laboratory<br/>General laboratory equipment<br/>The individual bench<br/>Equipment for parallel experiments<br/>Equipment for controlled experimentation<br/><br/>Purification and drying of solvents<br/>Introduction<br/>Purification of solvents<br/>Drying agents<br/>Drying of solvents<br/>References<br/><br/>Reagents: Preparation, purification, and handling<br/>Introduction<br/>Classification of reagents for handling<br/>Techniques for obtaining pure and dry reagents<br/>Techniques for handling and measuring reagents<br/>Preparation and titration of simple organometallic reagents and lithium amide bases<br/>Preparation of diazomethane<br/>References<br/><br/>Gases<br/>Introduction<br/>Use of gas cylinders<br/>Handling gases<br/>Measurement of gases<br/>Inert gases<br/>Reagent gases<br/>References<br/><br/>Vacuum pumps<br/>Introduction<br/>House vacuum systems (low vacuum)<br/>Medium vacuum pumps<br/>High vacuum pumps<br/>Pressure measurement and regulation<br/><br/>Carrying out the reaction<br/>Introduction<br/>Reactions with air-sensitive reagents<br/>Reaction monitoring<br/>Reactions at other than room temperature<br/>Driving equilibria<br/>Agitation<br/>Use of controlled reactor systems<br/>References<br/><br/>Working up the reaction<br/>Introduction<br/>Quenching the reaction<br/>Isolation of the crude product<br/>Data that need to be collected on the crude product prior to purification<br/><br/>Purification<br/>Introduction<br/>Crystallization<br/>Distillation<br/>Sublimation<br/>Flash chromatography<br/>Dry-column flash chromatography<br/>Preparative TLC<br/>Medium pressure and prepacked chromatography systems<br/>Preparative HPLC<br/>References<br/><br/>Small-scale reactions<br/>Introduction<br/>Reactions at or below room temperature<br/>Reactions above room temperature<br/>Reactions in NMR tubes<br/>Purification of materials<br/><br/>Large-scale reactions<br/>Introduction<br/>Carrying out the reaction<br/>Workup and product isolation<br/>Purification of the products<br/><br/>Special procedures<br/>Introduction<br/>Catalytic hydrogenation<br/>Photolysis<br/>Ozonolysis<br/>Flash vacuum pyrolysis (FVP)<br/>Liquid ammonia reactions<br/>Microwave reactions<br/>References<br/><br/>Characterization<br/>Introduction<br/>NMR spectra<br/>IR spectra<br/>UV spectroscopy<br/>Mass spectrometry<br/>Melting point (m.p.) and boiling point (b.p.)<br/>Optical rotation<br/>Microanalysis<br/>Keeping the data<br/><br/>Troubleshooting: What to do when things don’t work<br/><br/>The chemical literature<br/>The structure of the chemical literature<br/>Some important paper-based sources of chemical information<br/>Some important electronic-based sources of chemical information<br/>How to find chemical information<br/>Current awareness<br/>References<br/><br/>Appendices<br/>Properties of common solvents<br/>Properties of common gases<br/>Approximate pKa values for some common reagents versus common bases<br/>Common Bronsted acids<br/>Common Lewis acids<br/>Common reducing reagents<br/>Common oxidizing reagents<br/><br/>Index<br/><br/> |
| 520 ## - SUMMARY, ETC. |
|---|
| Summary, etc |
With an emphasis on the most up-to-date techniques commonly used in organic synthesis, this third edition reference draws on the extensive experience of the authors and their association with some of the world' s leading laboratories of synthetic organic chemistry. Written mainly for postgraduate, advanced undergraduate, and industrial organic chemists, this book emphasizes understanding rather than learning facts and offers fully updated information and re-drawn figures to illustrate the information at the highest possible standard. The increased size ...<br/> |
| 650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM |
|---|
| Topical term or geographic name as entry element |
Organic compounds |
| General subdivision |
Synthesis. |
| 650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM |
|---|
| Topical term or geographic name as entry element |
Chemistry, Organic |
| Form subdivision |
Laboratory manuals. |
| 700 1# - ADDED ENTRY--PERSONAL NAME |
|---|
| Personal name |
Lygo, B., |
| Relator term |
author. |
| 700 1# - ADDED ENTRY--PERSONAL NAME |
|---|
| Personal name |
Procter, Garry, |
| Relator term |
author. |
| 906 ## - LOCAL DATA ELEMENT F, LDF (RLIN) |
|---|
| a |
7 |
| b |
cbc |
| c |
origcop |
| d |
2 |
| e |
ncip |
| f |
20 |
| g |
y-gencatlg |
| 942 ## - ADDED ENTRY ELEMENTS (KOHA) |
|---|
| Source of classification or shelving scheme |
Dewey Decimal Classification |
| Koha item type |
Books |