TY - BOOK AU - Pavia,Donald L TI - Introduction to organic laboratory techniques: small-scale approach T2 - Saunders golden sunburst series SN - 0030245192 AV - QD261 .I543 1998 U1 - 547.0078 21 PY - 1998///] CY - Fort Worth PB - Saunders College Pub. KW - Chemistry, Organic KW - Laboratory manuals KW - fast N1 - Includes bibliographical references and index; Part 1 Preparations and reactions of organic compounds: isolation of the active ingredient in an analgesic drug; acetylsalicylic acid; acetanilide; acetaminophen; isolation of caffeine; TLC analysis of analgesic drgus; ethanol from sucrose; isopentyl acetate (banana oil); preparation of a C-4 or C-5 acetate ester; methyl alicylate oil (oil of methyl oleate); preparation of soap; preparation of a detergent; N, N-diethyl-m-toluamide - the insect repellent "OFF"; gas chromatographic analysis of gasolines; isolation of essential oils from allspice, cloves, cumin, caraway, cinnamon or fennel; thin=layer chromatography for monitoring the oxidation of borneol to camphor; an oxidation-reduction scheme. (Part contents.) N2 - This laboratory text for students of organic chemistry is designed to utilize standard-scale (macroscale) glassware and equipment but with smaller amounts of chemicals and reagents. It features a number of traditional organic reactions and syntheses, along with the isolation of natural products ER -