TY  - BOOK
AU  - Siddiqui,Anees Ahmad
TI  - Organic Medicinal Chemistry: practical Manual for Pharmacy and Science Students 
SN  - 9789387085145
U1  - 615.19 23
PY  - 2018///
CY  - New Delhi
PB  - CBS Publishers & Distiributors, 
KW  - Chemistry, Organic
KW  - Pharmaceutical chemistry
N1  - Includes Index; BASIC CHEMISTRY LAB EQUIPMENT Heating Devices -- Magnetic Stirrer -- Fumehood -- COMMON LABORATORY TECHNIQUES Handling of Glassware -- Heating Sources -- Filtration -- Decolourization -- Refluxing -- Sublimation -- Chromatography -- Solvent Drying and Drying Agents -- Use of Conventional Drying Agents -- Drying Process of Some Common Solvents -- TRAPS -- Simple Distillation -- Calculation of Percent Yield -- Theoretical, Actual and Percent Yields -- 3. CRYSTALLIZATION TECHNIQUE Selection of a Suitable Solvent for the Recrystallization -- Dissolving the Impure Solid in a Minimum Volume of Hot Solvent -- Removal of Any Insoluble Impurities by Filtration -- Crystallization of the Desired Compound from the Solution -- Isolation of the Purified Solid Compound -- DETERMINATION OF MELTING AND BOILING POINTS Determination of Melting Point -- Determination of Boiling Point -- SINGLE STEP SYNTHESIS --; Experiment 5.1: Synthesis of Aspirin (Acetyl Salicylic Acid) from Salicylic Acid -- Experiment 5.2: Synthesis of 2,4,6-Tribromophenol from Phenol -- Experiment 5.3: Synthesis of Picric Acid from Phenol -- Experiment 5.4: Synthesis of Urotropine from Formaldehyde -- Experiment 5.5: Synthesis of Phenyl Benzoate from Phen? -- Experiment 5.6: Synthesis of 2,3-Dihydro-1,4-Phthalazinedione from Phthalic Anhydride -- Experiment 5.7: Synthesis of Methyl Salicylate (Oil of Wintergreen) from Salicylic Acid -- Experiment 5.8: Synthesis of m-Dinitrobenzene from Nitrobenzene -- Experiment 5.9: Synthesis of Dibenzalacetone from Acetone -- Experiment 5.10: Synthesis of 2,4,6-Tribromoaniline from Aniline -- Experiment 5.11: Synthesis of 1,2,3,4-Tetrahydrocarbazole from Cyclohexanone  -- Experiment 5.12: Synthesis of 7-Hydroxycoumarin (Umbelliferone) -- Experiment 5.13: Synthesis of 2,4,5-Triphenyl IH-Imidazole from Benzil -- Experiment 5,14: Synthesis of Benzylideneaniline (Schiff Base) from Aniline -- Experiment 5.15: Synthesis of 2-Naphthol Aniline or Aniline Yellow Dye -- Experiment 5.16: Synthesis of lodoform from Ethyl Alcohol or Acetone -- Experiment 5.17: Synthesis of Benzoic Acid from Benzamide -- xperiment 5.18: Synthesis of Benztriazole from o-Phenylenediamine -- Experiment 5.19: Synthesis of Benzimidazole from o-Phenylenediamine -- Experiment 5.20: Synthesis of 2-Phenyl-4H-Benzo[1,3] Oxazin-4-one from Anthranilic Acıd -- Experiment 5.21: Synthesis of 3,5-Dimethyl Pyrazole from Acetylacetone -- Experiment 5.22: Synthesis of 2,5-Diphenyl Oxazole -- Experiment 5.23: Synthesis of Chalcone (Benzal Acetophenone) -- Experiment 5.24: Synthesis of m-Nitrobenzoic Acid from Benzoic Acid -- Experiment 5.25: Synthesis of Barbituric Acid from Urea -- Experiment 5.26: Synthesis of a-Phenylthiourea from Aniline --Experiment 5.27: Synthesis of Glucosazone from Glucose -- Experiment 5.28: Synthesis of Anthrone from Anthraquinone -- Experiment 5.29: Synthesis of Phenolphthalein from Phthalic Anhydride and Phenol -- Experiment 5.30: Synthesis of Benzocaine from para-Aminobenzoic Acid -- Experiment 5.31: Synthesis of Benzanilide from Aniline -- Experiment 5.32: Synthesis of Chlorobutanol from Acetone and Chloroform -- Experiment 5.33: Synthesis of Acetaminophen from p-Aminophenol -- Experiment 5.34: Synthesis of Phenothiazine from Diphenylamine -- Experiment 5.35: Synthesis of Phenacetin from Acetaminophen -- Experiment 5.36: Synthesis of 1-Phenyl-3-Methylpyrazol-5-one from Phenyl Hydrazine -- Experiment 5.37: Synthesis of Hippuric Acid from Glycine -- Experiment 5.38: Synthesis of 2,5-Dimethyl-1-Phenyl Pyrole from 2,5-Hexanedione I17 Experiment 5.39: Synthesis of Benzoic Acid (and Benzyl Alcohol) from Benzaldehyde -- Experiment 5.40: Synthesis of 5-Nitro Salicylic Acid from Salicylic Acid --Experiment 5.41: Synthesis of Cinnamic Acid from Benzaldehyde -- 6. TWO STEP SYNTHESIS Experiment -- 6.1: Synthesis of p-Bromoacetanilide from Aniline -- Experiment 6.2: Synthesis of p-Nitroacetanilide from Aniline -- Experiment 6.3: Synthesis of 4-Methyl-7-Acetoxycoumarin from Resorcinol -- Experiment 6.4: Synthesis of 9-Acridone from o-Chlorobenzoic Acid -- Experiment 6.5: Synthesis of 4-Benzylidene-2-Methyloxazole-5-one from Glycine -- Experiment 6.6: Synthesis of Dilantin (5,5-Diphenyl Hydantoin) from Benzoin -- Experiment 6.7: Synthesis of Anthranilic Acid from Phthalic Anhydride -- Experiment 6.8: Synthesis of 2-Phenylindole from Acetophenone -- Experiment 6.9: Synthesis of Benzilic Acid from Benzoin -- Experiment 6.10: Synthesis of 2,3-Diphenyl Quinoxaline from Benzil and b-Phenylenediamine -- Experiment 6.11: Synthesis of 6-Methoxy-2-Amino Benzothiazole from 6-Methoxy-2-Aniline -- Experiment 6.12: Synthesis of 4-Phenyl Butyric Acid from Benzene via Friedel Craft Reaction -- Experiment 6.13: Synthesis of Caprolactam from Cyclohexanone -- Experiment 6.14: Synthesis of Propranalol from a-Naphthol -- Experiment 6.15: Synthesis of Isatin from Aniline -- Experiment 6.16: Synthesis of Lidocaine from 2,6-Dimethyl Aniline -- Experiment 6.17: Synthesis of Methyl Orange from Aniline -- Experiment 6.18: Synthesis of Eosin from Resorcinol -- 7. MULTI STEP SYNTHESIS -- Experiment 7.1: Synthesis of Flavone from 2-Hydroxy Acetophenone -- Experiment 7.2: Synthesis of p-Bromoaniline from Aniline -- Experiment 7.3: Synthesis of Sulphanilamide from Aniline -- Experiment 7.4: Synthesis of N-Phenyl Succinimide from Succinic Acid -- Experiment 7.5: Synthesis of Tolbutamide from Toluene -- 8. EXTRACTION PROCEDURE -- Experiment 8.1: Extraction of Caffeine from Tea Leaves -- Experiment 8.2: Isolation of L-Cystine from Human Hairs -- Experiment 8.3: Extraction of Carvone from Caraway Seeds -- Experiment 8.4: Isolation of Limonene from Orange Peel -- Experiment 8.5: Isolation of Eugenol from Clove Buds -- Experiment 8.6: Isolation of Citric Acid from Lemon Juice -- Experiment 8.7: Isolation of Nicotine from Tobacco Leaves -- Experiment 8.8: Isolation of Piperine froh Pepper -- Experiment 8.9: Extraction of Casein from Milk -- Experiment 8.10: Isolation of Lactose from Powdered Milk -- Experiment 8.11: Isolation of Lycopene from Tomato -- Experiment 8.12: Isolation of Trimyristin from Nutmeg -- Experiment 8.13: Isolation of Quercetin from the Leaves of Fenugreek (Trigonella Foenum) -- SECTION III 9. ORGANIC NAME REACTIONS --  VIVA VOCE QUESTIONS -- INDEX
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